An organic material N-methyl-4-nitroaniline (NMNA) has been grown by the slow evaporation technique at ambient temperature. The grown NMNA crystal crystallized using three different solvents such as tetrahydrofuran (THF), dimethylsulfoxide (DMSO) and acetone, respectively. The grown crystal system and crystallinity were determined by single crystal and powder X-ray diffraction (XRD) analysis. F...

Neste trabalho substâncias húmicas (SH) extraídas de solos não alagáveis (Araçá) e alagáveis (Iara) foram caracterizadas com cálculos de estabilidade e energias de ativação associadas com a desidratação e decomposição térmica de SH utilizando TGA and DTA, ressonância paramagnética eletrônica (EPR) e razões atômicas C/H, C/N e C/O. Para SH extraídas de solos alagáveis, existe evidências da influ...

This paper reports on the synthesis of Cannabis indica fiber-reinforced composites using Urea-Resorcinol-Formaldehyde (URF) as a novel matrix through compression molding technique. The polycondensation between urea, resorcinol, and formaldehyde in different molar ratios was applied to the synthesis of the URF polymer matrix. A thermosetting matrix based composite, reinforced with lignocellulose...

A new organic nonlinear optical (NLO) material L-Histidinium trifluoroacetate was crystallized using LHistidine and trifluoroacetic acid in 1:1 stoichiometric ratio in water-ethanol medium. X-ray diffraction analysis of the single crystals showed that they belong to triclinic system, space group P1, with two molecules per unit cell. The lattice parameters are a = 5.1673(2) Å, b = 8.8393(3) Å, c...

The capacity for secondary effluent filtration of hollow fiber polypropylene membranes grafted with several zwitterionic molecules and multi-walled carbon nanotubes was evaluated. In particular, all the modifications result in significant improvement of filtration performances. The anti-fouling properties of the membrane had been increased without damaging the membrane as observed from FTIR, TG...

Graft copolymerization of acryl-amide onto guar-gum has been carried out in the presence of potassium per sulphate as a redox initiator. The prepared graft copolymer was characterized by various techniques such as FT-IR, SEMEDX and TGA-DTA-DTG. Activated charcoal was also studied as the adsorbent in the present study to evaluate their adsorption capacity for Cr (Vl) and compared it with indigen...

The [Co(Me(2)Salen)(PBu(3))(OH(2))]BF4 and [Co(Me(2)Salen)(PPh(3))(Solv)]BF(4), complexes were synthesized and characterized by FT-IR, UV-Vis, (1)H NMR spectroscopy and elemental analysis techniques. The coordination geometry of [Co(Me(2)Salen)(PPh(3))(H(2)O)]BF(4) was determined by X-ray crystallography. It has been found that the complex is containing [Co(Me(2)Salen)(PPh(3))(H(2)O)]BF(4) and ...

The mechanical stability is an important phenomenon which governs many applications based properties of membranes. The inorganic materials of membrane may have been synthesized by qualitative the novel sol-gel or co-precipitation methods of material synthesis. The mMembranes of cobalt (CP) and nickel (NP) composites have been was designed by mixing of the polyvinyl chloride (PVC) with cobalt ph...