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در این کار پژوهشی، نمونههای هیدروکسی اپتایت آلاییده با ناخالصیهای سریم، گادولونیم و ترکیبی از دو ناخالصی به روش هیدروترمال سنتز شدند. منظور بررسی فازهای بلوری تشکیل یافته هرکدام شده، کد MAUD که یک نرمافزار برای تجزیه تحلیل ساختار ماده استفاده پراش بر اساس ریتولد است، شد. پاسخ دزیمتری ترمولومینسانس نمونهها مورد قرار گرفت یافتهها نشان داد نمونه ترکیبی، سطح میانی است. مشخص شد افزودن سریم می...
Enhancing Materials and Device Analysis Capability in the SEM and FIB-SEM by using a Nanomanipulator
Nanomanipulators, whilst commonly used to lift out TEM samples prepared in the FIB, have a number of other potential applications and can aid in the chemical and crystallographic analysis of samples. Here, we discuss some of these alternative uses of nanomanipulators and show how they enable the EDS and EBSD analysis of thin samples in the FIB-SEM as well as serve as electrical probes and enabl...
The microstructure evolution of electroplated copper films was characterized by electron backscatter diffraction (EBSD). Special care was taken during the preparation of the cross-sectional specimens and microstructure analysis to obtain reliable results. The film exhibited a columnar grain structure with a large fraction of twin boundaries. Annealing induced normal grain growth and caused many...
transformation induced plasticity (trip) steels have a vast application in automotive industry because of theirhigh strength, high ductility and hence excellent energy absorption capacity. these characteristics of tripsteels are due to the existence of retained austenite in their microstructures in the ambient temperature, whichtransforms to the martensite phase during deformation. the microstr...
Electron BackScatter Diffraction (EBSD) in conjunction with Field-Emission Environmental Scanning Electron Microscopy (FEG-ESEM) has been used to evaluate the microstructural and local plastic strain evolution in different alloys (AISI 1005, AISI 304L and Duplex 2205) deformed by a single-stage cold and warm forging process. The present work is aimed to describe the different behavior of the au...
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