نتایج جستجو برای: x ray structural analysis
تعداد نتایج: 3630095 فیلتر نتایج به سال:
A room temperature solid-state structural transformation was observed in 3 nm ZnS nanoparticles in methanol following the addition of water (Zhang et al., Nature 424, 1025, 2003). Experimental wide angle x-ray scattering (WAXS), x-ray absorption near edge structure (XANES) and extended x-ray absorption fine structure (EXAFS) spectroscopy measurements show a large increase in crystallinity assoc...
In this paper, Ni-doped lead hexaferrites (PbFe12-xNixO19) nanoparticles with x = 0.2 were prepared by sol- gel method. Then, the effect of annealing temperature on its structural, magnetic and dielectric properties was studied. First, the dryed gel was evaluated by Thermogravimetry-Differential Thermal Analysis (TG/DTA) and then, the structural morphology, magnetic and dielectric properties of...
We present a robust data analysis method of time-resolved x-ray absorption spectroscopy experiments suitable for chemical speciation and structure determination of reaction intermediates. Chemical speciation is done by principal component analysis (PCA) of the time-resolved x-ray absorption near-edge structure data. Structural analysis of intermediate phases is done by theoretical modeling of t...
condensation of glyoxal, formaldehyde and anilines lead to the formation of 2,4,6,8- tetraphenyl and substituted phenyl 2,4,6,8-tetraazabicyclo [3.3.0] octanes. the reactions are sensitive to ph and temperature. ortho derivatives of anilines do not participate in this condensation. x-ray structural determination reveals a cis-dienvelope geometery about the two fused rings.
The highly successful scattering density profile (SDP) model, used to jointly analyze small-angle X-ray and neutron scattering data from unilamellar vesicles, has been adapted for use with data from fully hydrated, liquid crystalline multilamellar vesicles (MLVs). Using a genetic algorithm, this new method is capable of providing high-resolution structural information, as well as determining bi...
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