نتایج جستجو برای: x ray analysis
تعداد نتایج: 3355651 فیلتر نتایج به سال:
Oxide nanoparticles can exhibit unique physical and chemical properties due to their limited size and a high density of corner or edge surface sites. In this study, MgO nanoparticle was synthesized using Mg(CH3COO)2 and hexamethylenetetramine as starting materials. The structure and optical properties of these particles are investigated by using X-ray diffraction (XRD), sc...
X-ray diffraction (XRD) technique is commonly used for qualilative ana lysis of minerals, and has also been successfully used for quantitative measurements. In this research, the matrix fl ushing and a new X-ray diffraction method have been used for the determination of crystallinity and amorphous content of Opal and Quartz mixture. The PCAPD is used to detemline the quanti tative analysi...
lta zeolite nanoparticles was successfully synthesized from clear solution under controlled conditions using hydrothermal method using tetramethyl ammonium hydroxide as a structural directing agent. the as-synthesized lta zeolite particles were characterized by powder x-ray diffraction (xrd) analysis, scanning electron microscopy (sem), fourier transform infrared (ft-ir) spectroscopy, energy di...
o bjectives: this study aimed to compare a number of new nanocomposites capable of pro- tecting the jaw from ionizing radiation. mat erials and methods: four different types of nano-powders [ti, zr (iv) oxide, ag and co] were mixed in a polymer matrix to create nano-composites with doping values of 8% in weight. small-angle x-ray scattering (saxs) analysis was performed using a hecus- saxs syst...
Oxide nanoparticles can exhibit unique physical and chemical properties due to their limited size and a high density of corner or edge surface sites. In this study, MgO nanoparticle was synthesized using Mg(CH3COO)2 and hexamethylenetetramine as starting materials. The structure and optical properties of these particles are investigated by using X-ray diffraction (XRD), sc...
Two nano-sized mixed-ligand Cd (II) coordination polymers; [Cd (4,4' -bpy) (C4H4O4)].1/4 H2O (1) and[Cd(bpy)1.5 (NO3)2].3H2O (2) (bpy=bipiridine) were synthesized by a sonochemical method and characterized by elemental analyses, thermal gravimetric analysis (TGA), differential thermal analysis (DTA), scanning electron microscopy (SEM) and Fourier transform infrared spectroscopy (FT-IR). The cry...
لیگاند 5- برومو-سالیسیلیدین-ایمین-n,n دی متیل-اتیلن آمین، از واکنش 5- برومو-سالیسیل آلدهید و n,n- دی متیل-اتیلن دی آمین در حلال متانول و طی چهار ساعت تقطیر برگشتی تهیه گردید. سپس این لیگاند با اکسید وانادیوم(iv) استیل استونات، استات مس(ii) یک آبه، استات روی(ii) دو آبه و نیترات نیکل(ii) شش آبه با نسبت 1:2 و در حلال متانول به مدت دو ساعت واکنش داده، که به ترتیب کمپلکس-های[vol(acac)] ، [cu2l2(oac)...
کمپلکس [ptme(ppy)pph3]- فنیل پیریدینppy = 2 با( bix3( x= cl, br, i واکنش میدهد و محصولات cis-[ptme(x)2(ppy)pph3],3a, x=cl,3b, x= br, 3c, x= iوpt(x(ppy)pph3] 2b,x= i,2a,x=cl, بدست می آیند. برای اثبات محصول واکنش کمپلکس [ptme(ppy)pph3] با bii3 واکنش کمپلکس (pt(ii با i2 انجام شد و داده های به دست آمده از این واکنش با واکنش با bii3 در حلال مشابه مقایسه شد. این کمپلکس ها با طیف سنجی 1hnmr , 31pnmr و...
titanium nitride-copper (tin-cu) nanocomposite films were deposited onto stainless steel substrate using hollow cathode discharge ion plating technique. the influence of cu content in the range of 2-7 at.% on the microstructure, morphology and mechanical properties of deposited films were investigated. structural properties of the films were studied by x-ray diffraction pattern. topography of t...
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