Abstract The crystal structures of the pyribencarb E and Z stereoisomers were determined using single-crystal X-ray crystallography. isomers confirmed a single data respectively by analysis, LC-UVD mass spectrometry, NMR spectroscopy. Pyribencarb crystallizes in triclinic P − 1 isomer monoclinic 2 / c, with showing comparable packing motifs. Moreover, molecular docking was carried out cytochrom...

A 1:1 co-crystal of rac-trans-1,2-C(6)H(10)(OH)(2) and (C(6)H(5))(3)PO has been found that is unusual because there are no strong interactions between the two kinds of molecules, which are segregated into layers. Furthermore, neither pure rac-1,2-cyclohexanediol (CHD) nor pure triphenylphosphine oxide (TPPO) has any obvious packing problem that would make the formation of inclusion complexes li...

The crystal structures of 4-(4-methylphenyl)-6-phenyl-2,3,3a,4-tetrahydro-1H-pyrido[3,2,1-jk]carbazole (IIa) and 4-(4-methoxyphenyl)-6-phenyl-2,3,3a,4-tetrahydro-1H-pyrido[3,2,1-jk]carbazole (IIb) were elucidated by single crystal X-ray diffraction. Compound (IIa), C28H25N, crystallizes in the triclinic system, space group P-1, with a = 8.936(2) Å, b = 10.490(1) Å, c = 11.801(1) Å, α = 102.69(5...

The title crystal structure is a new triclinic polymorph of [(Ph3P)2N]Cl·(B(OH)3) or C36H30NP2 (+)·Cl(-)·BH3O3. The crystal structure of the ortho-rhom-bic polymorph was reported by [Andrews et al. (1983 ▶). Acta Cryst. C39, 880-882]. In the crystal, the [(Ph3P)2N](+) cations have no significant contacts to the chloride ions nor to the boric acid mol-ecules. This is indicated by the P-N-P angle...

The synthesis and crystal structure of the one-dimensional coordination polymer, [Cd(spar)2]n·n(H2O), are described, where spar is the sparfloxacinate anion, C19H21N4O3F2. The Cd ion is bonded to four spar ligands: Two O,O-chelate with their β-keto carboxylate groupings and two are monodentate-bound through a carboxylate O atom, to result in a distorted CdO6 octahedral coordination geometry. Th...

Zinc (II) complex, [Zn(25-MBTSC)2I2] (1), where (25-MBTSC = (E)-2-(2,5-dimethoxybenzaldehyde) thiosemicarbazone, has been synthesized from the reaction of ZnI2 with 25-MBTSC in methanol as solvent at 25 ºC. It was characterized by elemental analysis (CHN) and is confirmed by single-crystal X-ray diffraction analysis. The complex 1 crystallizes in a triclinic system, with space group P-ī, having...

A novel complex Ni(C 12 H N 2 ) 3 ●(C 7 5 O ●(H BO has been synthesized from a hydrothermal reaction and the crystal structure determined by means of single-crystal X-ray diffraction. Triclinic, P-1. a= 12.5380(13) Å, b = 13.0100(15) c 15.1490(18) α= 102.760(3)°, β= 94.480(2)°, γ= 94.540(2)°. V=2390.9(5) Å3. Z=2. R 1 =0.0661, wR 0.2128, T=293(2) K. The Ni atom is coordinated six atoms three 4,4...

This paper covers nineteen Pt(II) complexes of the composition Pt(η3-X1X2X3)(PR3), (X = N1, N2, N3; S1, S2, S3; or Te1, Te2, Te3). These crystallized in three crystal classes: triclinic (eleven examples), monoclinic (six and orthorhombic (two examples). Each tridentate ligand creates two metallocyclic rings with common Te2 donor ligands types N1C2N2C2N3, N1C2N2NC2N3, S1C2S2C2S3, S1C3S2C3S3, Te1...