Nano Bioactive glass material of the type CaO–P2O5–SiO2 was obtained by the sol-gel processing method at considerably lower temperatures than required for conventional melting methods. As a new modification, volume of solution was changed in order to investigate its effects on the properties of bioglass samples. The obtained material was characterized by X-ray powder diffraction (XRD), surface ...

To improve the corrosion protection of copper metal, 0.01M concentration of 1H-1,2,4-triazole-3-thiol (TAT) was incorporated into the hybrid sol-gel monolayers containing 3-glycidoxypropyltrimethoxysilane (GPTMS) and Tetraethoxysilane (TEOS). It was further subjected to hydrolysis and condensation reaction to form a sol-gel matrix. The TAT-doped hybrid sol-gel coating was applied over the c...

polyimide/nickel oxide (polyimide/nio) nanocomposite was successfully synthesized by sol gel technique, using pyromellitic dianhydriede (pmda), 4,4-oxydianiline (oda) and n,n-dimethylacetamide (dmac) and 10 wt% nickel titanate nanopowders (nps). fourier transform infrared spectrometry (ftir), x-ray diffraction (xrd), scanning electron microscopy (sem), and vibrating sample magnetometer (vsm) we...

objective(s): hardystonite (ht) has been successfully prepared by a modified sol-gel method. we hypothesized thatnano-sized (ht) would mimic more efficiently the nanocrystal structure and function of natural bone apatite, owing to the higher surface area, compare to conventional micron-size (ht).materials and methods: the hardystonite nanopowder was prepared via a modified sol-gel method.optimi...

Nano Bioactive glass material of the type CaO–P2O5–SiO2 was obtained by the sol-gel processing method at considerably lower temperatures than required for conventional melting methods. As a new modification, volume of solution was changed in order to investigate its effects on the properties of bioglass samples. The obtained material was characterized by X-ray powder diffraction (XRD), surface ...

zinc ferrite (znfe2o4) nanoparticles were synthesized via the auto-combustion assisted sol-gel method of zn2+ and fe3+ ions (molar ratio 1:2) in ammonia solution. the prepared nanomagnetic catalyst was characterized by ir, xrd, sem and icp. the diameter of the znfe2o4 mnps (63.7 nm) was determined by debye-scherre equation via their xrd pattern. nanomagnetic znfe2o4 efficiently catalyzes oxidat...

The silica supported platinum nanoparticles was synthesized by using the sol-gel method. The possibility of using diamminedinitro platinum (II) as Pt precursor and effect of metal precursor concentration on the final Pt nanoparticle size was investigated. A stable silica sol was prepared via hydrolysis of tetraethyl orthosilicate (TEOS) as a metal alcoxide and condensation reaction. Subsequentl...

Using PVDF and ZrO2, polymer composites were prepared by sol gel method. Various measurements such as X-ray diffraction (XRD), Scanning electron microscopy (SEM) and Differential Scanning Calorimetry (DSC) were used to characterize the composites. Thermal and electrical properties of the composite samples were studied. The conductivity of composites was found to increase with increase in temper...

Calcium doped nickel ferrite powders have been prepared by sol-gel combustion technique. Metal nitrates, such as calcium nitrate, nickel nitrate and ferric nitrate, were used as the source materials and citric acid and polyvinyl alcohol were used as the burning agent and agglomeration reducing agent, respectively. The average crystallite size of the prepared ferrite was in the order of ~70- 92 ...

Calcium doped nickel ferrite powders have been prepared by sol-gel combustion technique. Metal nitrates, such as calcium nitrate, nickel nitrate and ferric nitrate, were used as the source materials and citric acid and polyvinyl alcohol were used as the burning agent and agglomeration reducing agent, respectively. The average crystallite size of the prepared ferrite was in the order of ~70- 92 ...