A simple spectrophotometric method is developed for the determination of phosphate in sugar cane juice, water and detergent samples. The method is based on the formation of phosphomolybdate with added molybdate followed by its reduction with sodium sulphide in aqueous sulfuric acid medium. The system obeys Lambert-Beer’s law at 715 nm in the concentration range 0.3-12.24 ppm. Molar absorptivity...

Manure pits and silos are potentially dangerous, gas-containing confined spaces on the farm that may generate hazardous levels of hydrogen sulphide and nitrogen dioxide respectively. Although these inhalation injuries are uncommon, emergency physicians who work within transport distance of rural areas should be aware of the toxic agents involved and their acute management. This article reviews ...

In this work we report the synthesis and characterization of hybrid nanostructures of multiwall carbon nanotubes (MWCNT) and cadmium sulphide (CdS) nanoparticles. In a solution of thioacetamide and cadmium sulphide, purified MWCNT are added to prepare the CNT/CdS hetrostructure. XRD diagrams, SEM images, and also photoluminescence spectra of the prepared samples are analyzed. SEM images show th...

In this paper we report on ZnS nanoparticles produced by precipitation of zinc acetate and sodium sulphide and stabilized by cetyltrimethylammonium bromide (CTAB) in aqueous media and deposited on montmorillonite (MMT). For the deposition a new method based on intensive cavitation was used. The montmorillonite carrier was first disintegrated by intense turbulent mixing in an ultrasonic field in...

Some novel 4-(aryliidineamino)-5-(1-(4-isobutylphenyl) ethyl)-4-yl-4H-1,2,4-triazole-3-thiols were prepared from the reaction of carbon-di-sulphide and hydrazine hydrate in water to produce thiocarbohydrazides. The thiocarbohydrazides is then refluxed with ibuprofen for 2 hour, followed by cooling to room temperature and washing with sodium bicarbonate solution to produce 5-(1-(4isobutylphenyl)...

Different samples of ZnS nanoparticals were synthesized by chemical co-precipitation method at room temperature using zincsulphate as zinc source and sodium sulphide as sulphur source. Structural properties of synthesized ZnS nanoparticles were studied by X-ray diffraction pattern (XRD) while optical properties were examined by UV-Visible absorption spectroscopy. XRD pattern showed the as synth...

In this study, grinding + flotation experiments were performed on the sample of complex Pb-Zn sulphide ore taken from Niğde (Ulukışla-Madenköy) region in Turkey. According to mineralogical analysis used experimental studies, it was determined that composition contains calcite, quartz, pyrite, chalcopyrite, hematite, goethite, limonite, gypsum, galena, sphalerite, jarosite, arsenopyrite and marc...

Benzotiazole and pyrimidine have been reported to act as effective pharmacophores. However, much less work as been carried out on these heterocycles fused with each other. In the present study, we report the synthesis of a series of 8-chloro-3(phenylcarbonoimidoyl)-10a-H-pyrimido [2,1-b][1,3]benzothiazole-2-thiol. This series was synthesized by the reaction of 8-chloro-2-sulfanyl-10a-H-pyrimido...

In surface sediments, metal mobility is controlled by the recruitment and turn-over of organic matter whereas sulphide is thought to control the concentration of metals in sediment pore water by removing them from the solution. DGT is a dynamic probe that measures the kinetically available fraction of metals or sulphide. DGT uses a credit card size probe inserted into the sediment that provides...

IUPAC name: Hydrogen sulphide Common name: Hydrogen sulphide CAS number: 7783-06-4 Synonyms: Dihydrogen monosulphide ; dihydrogen sulphide, hydrogen sulphuric acid ; sewer gas ; stink damp ; sulphuretted hydrogen ; sulphur hydrogen EINECS 231-977-3 EC number 016-001-00-4 Molecular formula : H2S Molecular weight: 34.09 Freezing point at 101.3 kPa: -85.5 C Boiling point at 101.3 kPa: -60.7 C Vapo...