A miniaturized pepsin reactor was prepared inside a fused-silica capillary (i.d. 75 microm) by coating a pepsin-containing gel on a photopolymerized porous silica monolith. The pepsin-encapsulated film was prepared by a sol-gel method. The sol-gel reaction was optimized so that the sol solution containing pepsin forms a thin film on the photopolymerized sol-gel (PSG) monolith that was initially...

Nanosized TiO2 particles were prepared by sol–gel method. The TiO2 particles were co-deposited with chromium using electrodeposition technique. In investigating of coating surfaces by scanning electron microscope (SEM), the results showed that the morphology of the coating surface was changed by adding TiO2 nanoparticles to the chromium coating. The corrosion behavior of the coatings was assess...

Soft lithography using polydimethylsiloxane (PDMS) allows one to fabricate complex microfluidic devices easily and at low cost. However, PDMS swells in the presence of many organic solvents significantly degrading the performance of the device. We present a method to coat PDMS channels with a glass-like layer using sol-gel chemistry. This coating greatly increases chemical resistance of the cha...

A comparative study of two coating methods on titanium (Ti) substrates, sol-gel and electrophoresis processes, was performed. Before coating, two different surface treatments were employed. The hydroxyapatite (HA) powder were characterized by infrared spectroscopy (FTIR) and X-ray diffraction (XRD) while coated samples were examined by using scanning electron microscopy (SEM) with energy disper...

The sol-gel synthesis process is a versatile method used to produce wide diversity of materials and being increasingly as surface modification alter porosity, wettability, catalytic activity, biocompatibility corrosion performance underlying substrates. Silane sol–gel films deposited on aluminium alloys have been widely studied chemical conversion coatings coupling agent between the substrate o...

Transparent mesoporous silica films were prepared by sol-gel spin coating on silicon wafers at room temperature. An erbium complex, erbium tris 8-hydroxyquinoline (ErQ), was homogeneously impregnated into the pores of the mesoporous silica films, and its concentration was easily controlled by using a solution immersing technique. The ErQ-impregnated mesoporous silica films show a room-temperatu...

We explore the analytical performance and limitations of optically monitoring aqueous-phase temperature using protein-protected gold nanoclusters (AuNCs). Although not reported elsewhere, we find that these bio-passivated AuNCs show pronounced hysteresis upon thermal cycling. This unwanted behaviour can be eliminated by several strategies, including sol-gel coating and thermal denaturation of t...

ITO thin films were deposited by spin coating method starting from indium and tin propoxide in the frame of a sol-gel process. Films with the thickness corresponding to 68 nm for one layer deposition were produced and characterized by X-ray diffraction, transmission electron microscopy and infrared reflection spectroscopy. Low conductivity polycrystalline films exhibiting cubical structure (bix...

Abstract Sol–gel derived hydroxyapatite coatings on metallic implants are important to promote their osseointegration and biocompatibility. However, such generally suffer from drawbacks that limit implant longevity. In this study, the sol gel process prepare was optimized used deposit a layer Ti6Al4V. Samples were pretreated by thermal oxidation, sol–gel coating, anodization produce titanium di...