An efficient method for the synthesis of 5-substituted-1H-tetrazoles through the reaction of nitriles with sodium azide using titanium oxide–supported boric acid (TiO2-H3BO3) catalyst was reported. The reactions were carried out at 120 °C and provided the corresponding tetrazoles in good to excellent yields. This method displayed significant advantages ...

An efficient method for the synthesis of 5-substituted-1H-tetrazoles through the reaction of nitriles with sodium azide using titanium oxide–supported boric acid (TiO2-H3BO3) catalyst was reported. The reactions were carried out at 120 °C and provided the corresponding tetrazoles in good to excellent yields. This method displayed significant advantages ...

ZnO/SiO2 was prepared using sol-gel method, and vanadium particles were loaded on this nano-photocatalyst by wet incipient method. They characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), energy dispersive (EDX) analysis andFouriertransform infrared spectroscopy (FT-IR). The XRD patterns showed that the zinc oxide samples have a wurtzite structure and vanadium dope...

three high-silica mordenite zeolites differing in sio440, ratio were prepared by direct synthesis without using any template. the products si02/a120, ratio is influenced by the starting gel composition. this ratio is increased upon ion-exchange with nh,cl and subsequent calcination to prepare protonic mordenite. the protonic mordenites with si02/a1203ra tios of 14.6,29.2 and 34.6 were character...

the effect of rare earth (re) elements, including ce and la, on the sorption properties of zr-co getters was investigated in this work. the phase evolution, microstructural characteristics of getter powders were studied by means of x-ray diffraction method, scanning electron microscopy (sem) and energy dispersive x-ray spectroscopy (eds). the nanostructured zr3co intermetallic compound has been...

in this article vanadium boride nanopowder was synthesized by mechanochemical reduction method in a high-energy ball mill. the synthesized powders were studied by x-ray diffraction (xrd), scanning electron microscopy (sem), xray map and transmission electron microscopy (tem). according to x-ray diffraction the product predominantly consists of vb phases after 100 min milling without further hea...

Scanning electron microscopy/energy dispersive X-ray spectrometry (SEM/EDS) is a widely applied elemental microanalysis method capable of identifying and quantifying all elements in the periodic table except H, He, and Li. By following the "k-ratio" (unknown/standard) measurement protocol development for electron-excited wavelength dispersive spectrometry (WDS), SEM/EDS can achieve accuracy and...

The data presented in this article are related to the research article entitled: "Solder free joining as a highly effective method for making contact between thermoelectric materials and metallic electrodes" (Malik et al., 2017) [1]. This article presents microstructure obtained by scanning electron microscopy (SEM) and chemical analysis by energy dispersive X-ray spectroscopy (EDX) point measu...

sio2-coated cobalt ferrite (cofe2o4) nanoparticles were obtained by the hydrolysis of tetraethylorthosilicate in the presence of cofe2o4 nanoparticles in co-precipitation. the effects of sio2coating on the magnetic properties of cofe2o4 nanoparticles were investigated. the structural, morphological and magnetic properties of as-prepared sample were characterization by x-ray diffraction (xrd), f...

in this paper, the effect of magnetic field on the morphology, structure and magnetic properties of electrodeposited fecu/cu thin films was investigated. the films were deposited on au2pdag/glass substrates using electrodeposition technique in potentiostatic control. the magnetic fields of 5000 and 7000 oe were applied on deposition bath during deposition. two series of thin films were prepared...