In this article, we report a facile precursor pyrolysis by sol-gel method to prepare spinel-type Cobalt-substituted zinc aluminate nanoparticles (Zn1–xCoxAl2O4, 0 ? x 1). The relationship between the degree of crystallinity and optical properties under effect calcination temperature was investigated. synthesised powders were characterized means X-ray diffraction (XRD), Thermogravimetry Differen...

An efficient synthesis of 2,4,5-trisubstituted and 1,2,4,5-tetrasubstituted imidazoles by one-step condensation of  an aldehyde, benzil, ammonium acetate and primary amine in the presence of nanocrystalline magnesium aluminate under microwave irradiation is described. The advantages of this catalyst are including simple work-up, low cost and reusability. Compared with conventional methods, the ...

Porous monolithic catalysts with high specific surface areas, which can not only facilitate heat/mass transfer, but also help to expose active sites, are highly desired in strongly exothermic or endothermic gas-solid phase reactions. In this work, hierarchical spinel a porous woodpile architecture were fabricated via extrusion-based three-dimensional (3D) printing (direct ink writing, DIW brief...

Mineral wools are the most common insulation materials in buildings worldwide. However, mineral wool waste is often considered unrecyclable because of its fibrous nature and low density. In this paper, rock wool (RW) and glass wool (GW) were studied as alkali-activated material precursors without any additional co-binders. Both mineral wools were pulverized by a vibratory disc mill in order to ...

An efficient synthesis of 2,4,5-trisubstituted and 1,2,4,5-tetrasubstituted imidazoles by one-step condensation of  an aldehyde, benzil, ammonium acetate and primary amine in the presence of nanocrystalline magnesium aluminate under microwave irradiation is described. The advantages of this catalyst are including simple work-up, low cost and reusability. Compared with conventional methods, the ...

Oxygen isotopic measurements of 20 spinel (MgAl2O4) grains from the CM2 meteorite Murray (average diameter 0.45 m), seven spinel grains from ordinary chondrites (OC, 0.3 to 2 m) and three spinel grains from the CI chondrite Orgueil (0.4 to 0.7 m) have revealed large anomalies and thus established their presolar origin. Their O isotopic ratios fall into all four previously defined groups and ind...

In this study, cobalt aluminate was prepared by a sol-gel method. XRD and FTIR analyses of the precursors obtained at 300 °C for 12 h revealed that type complexing agent used in synthesis affects pyrolysis step. An amorphous phase using citric acid as agent. A beginning crystallization observed agents such polyacrylic glycine. The structural investigation starting reagents lines exhibit charact...

Three types of solvents with different polarity (cyclohexane, toluene and benzene), a nonionic surfactant Span 40 were used to prepare strontium aluminate (SrAl2O4) spinel nanoparticles by a reverse micelle method. The structure of SrAl2O4 nanoparticles was characterized by X-ray diffraction (XRD). The morphology and size of the synthesized materials were studied using field emission scanning e...