ABSTRACT: In this study, an analytical method is developed to determine 15 polycyclic aromatic hydrocarbons (PAHs) in olive and refined pomace olive oils using HPLC coupled with a fluorescence detector. The standardised method of ultrasound-assisted solvent extraction consisted of liquid–liquid extraction with organic solvent and purification on C18 and Florisil bonded-phase cartridges was modi...

The effects and influences of various operational parameters on the efficiency of mixer-settlers are thoroughly studied in this paper. One of the most important factors in designing a mixer-settler is to obtain an optimum operational extraction and overall efficiency. These two factors are dependent on various parameters such as impeller shape, size and speed of impeller, baffle size, residence...

Ion pair dispersive liquid- liquid microextraction (IP-DLLME) method combined with flame atomic absorption spectrometry was proposed for the determination of trace amounts of copper(II). By using pyrocatechol violet as chelating agent and cetyltrimethyl ammonium bromide as an ion pairing agent, the trace amount of copper(II) was extracted in chloroform. The factors influencing the formation cop...

Based on the importance of drops' behavior in liquid-liquid extraction, the maximum sauter mean drop diameter has been investigated and correlated in a counter-current spray extraction column with two chemical systems. Spargers were set of nozzles in all experiments. Studying the effects of several parameters on drops size, some correlations were estimated by the last available version of softw...

We report a liquid-liquid extraction system based on perfluorocarbon (fluorous-solvent extraction) that allows selective extraction of metal ions from aqueous and organic phases to a perfluorocarbon phase (FC-72) with perfluorinated beta-diketone (1,1,1,5,5,6,6,6-octafluoro-2,4-hexanedione), which can be followed by backward extraction using 1 M nitric acid.

Buprenorphine (BUP) is considered to be safe during pregnancy. However, the extent of BUP transfer into breast milk has not been investigated thoroughly. Because the drug concentration in the milk is 1 of the determinants in the assessment of the exposure risk, a rapid and sensitive LC-MS/MS method has been developed and evaluated to measure BUP and norbuprenorphine (norBUP) concentrations in m...

Microwave assisted extraction (MAE) tech-nique was employed for the extraction of pectin from black mulberry (Morus nigra) pomace in this research. The effects of process variables namely microwave power (300-900 watt), irradiation time (10-30 min) and liquid to solid ratio (15-30 mL/g) on the yield, degree of esterification (DE) and galacturonic acid content (GalA) of pectin were investigated ...

Microwave assisted extraction (MAE) tech-nique was employed for the extraction of pectin from black mulberry (Morus nigra) pomace in this research. The effects of process variables namely microwave power (300-900 watt), irradiation time (10-30 min) and liquid to solid ratio (15-30 mL/g) on the yield, degree of esterification (DE) and galacturonic acid content (GalA) of pectin were investigated ...

Microwave assisted extraction (MAE) tech-nique was employed for the extraction of pectin from black mulberry (Morus nigra L.) pomace in this research. The effects of process variables namely microwave power (300-900 watt), irradiation time (10-30 min) and liquid to solid ratio (15-30 mL/g) on the yield, degree of esterification (DE) and galacturonic acid content (GalA) of pectin were i...

Introduction: Fruit polysaccharides, essential health factors in foods, are widely present in edible fruits. Several methods for isolation of polysaccharide are available. Microwave Assisted Extraction (MAE) method is extensively used for separation of polysaccharides. Only little information is available about Psidium guajava L. Fruit Polysaccharide (PFP) and its extraction methods. Objective:...