Hard-magnetic nanomaterials like nanoparticles of FePt are of great interest because of their promising potential for data storage applications. The magnetic properties of FePt structures strongly differ whether the crystal phases are face centered cubic (fcc) or face centered tetragonal (fct). We evaluated aberration corrected HRTEM, electron diffraction and aberration corrected HAADF-STEM as ...

Despite the high potential of endohedral metallofullerenes (EMFs) for application in biology, medicine and molecular electronics, and recent efforts in EMF synthesis, the variety of EMFs accessible by conventional synthetic methods remains limited and does not include, for example, EMFs of late transition metals. We propose a method in which EMF formation is initiated by electron irradiation in...

Though tungsten trioxide (WO3) in bulk, nanosphere, and thin film samples has been extensively studied, few studies have been dedicated to the crystallographic structure of WO3 thin films. In this work, the evolution from amorphous WO3 thin films to crystalline WO3 thin films is discussed. WO3 thin films were fabricated on silicon substrates (Si/SiO2) by RF reactive magnetron sputtering. Once a...

A practical method for transmission electron microscopy specimen preparation of GaAs-based materials with quantum dot structures is presented to show that high-quality image observations in high-resolution transmission electron microscopy (HRTEM) can be effectively obtained. Specimens were prepared in plan-view and cross-section using ion milling, followed by two-steps chemical fine polishing w...

Magnetic tunnel junctions with an Fe3O4 top electrode have been fabricated. High resolution transmission electron microscopy (HRTEM) shows that in as-deposited state, Fe and FeO phases exist at the interface. These two phases are believed to have formed as a result of the unstable plasma condition at the start of the Fe3O4 deposition. A relatively low magnetoresistance ratio (MR) (3.5%) and low...

Porous high surface area thin films of nanosheet-shaped monoclinic MoO(3) were deposited onto platinized Si substrates using patch antenna-based atmospheric microplasma processing. The films were characterized by high resolution transmission electron microscopy (HRTEM), scanning electron microscopy (SEM) and electrochemical analysis. The electrochemical analysis shows original redox peaks and h...

We describe an approach allowing high-resolution transmission electron microscopy (HRTEM) on specimens like graphene and the investigation on their electronic transport properties at the same time. The experimental set-up presented here is based on the modification of a commercial TEM specimen holder and on a specially designed sample carrier. A customized Hall sensor confirms that the local ma...

Multiferroic bismuth ferrite (BiFeO(3)) nanotubes have been synthesized using a modified template methodology and characterized by a number of techniques, including XRD, SEM, TEM, HRTEM as well as EDX and SAED.

Continuous hydrothermal synthesis of metal oxide nanoand microparticles in supercritical water was performed in a continuous flow reactor. The results of investigation of LiCoO2, LiNiO2, LiZnO2, LiCuO2, Ga2O3, CeO2 nanoparticles by HRTEM and XRD analysis were presented.

The highly dispersed metal (e.g. Au) nanoparticles have exhibited exceptional catalytic activity for several reactions, including CO oxidation. Their high catalytic activity has been attributed to nanoparticles nano-structural effects (including cluster thickness, shape, chemical information, and number of atoms of the cluster). The three dimensional exact structure and chemical bonding state o...