The thermal stability of multiwalled carbon nanotubes (CNTs) was studied in high vacuum using tungsten nanoparticles as miniaturized thermal probes. The particles were placed on CNTs inside a high-resolution transmission electron microscope equipped with a scanning tunneling microscope unit. The setup allowed manipulating individual nanoparticles and heating individual CNTs by applying current ...

We prepared hydrazine-reduced materials from both graphite oxide (GO) particles, which were not exfoliated, and completely exfoliated individual graphene oxide platelets, and then analyzed their chemical and structural properties by elemental analysis, XPS, TGA, XRD, and SEM. Both reduced materials showed distinctly different chemical and structural properties from one another. While hydrazine ...

High-resolution CKa spectra have been obtained for samples containing carbon cage particles, synthesized using the arc-discharge graphite evaporation technique. The X-ray fluorescence spectrum of particles from the inner part of the cathode deposit was found to differ from that of the soot collected on the chamber walls. The dependence of the spectral profile on the geometry was investigated us...

Closed caged fullerene-like molybdenum disulfide (MoS2) nano-particles were obtained via an arc discharge between a graphite cathode and a molybdenum anode filled with microscopic MoS2 powder submerged in de-ionized water. A statistical study of over 150 polyhedral fullerene-like MoS2 nano-particles in plan view transmission electron microscopy revealed that the majority consisted of 2–3 layers...

Novel core-shell structure hard carbon/Si-carbon composites are prepared, and their electrochemical performances as an anode material for lithium-ion batteries reported. Three different types of shell coating applied using Si-carbon, Si-carbon black-carbon black-carbon/graphite nanosheets. It appears that the use n-Si/carbon black/carbon composite particles in place n-Si is great importance to ...

Graphitic Structures by Design (GSD) is a novel technology for growing graphite in precise patterns from the nano to the macroscale, rapidly (>1 layer/sec), at low temperatures (ca. 500C), and in a single step using ordinary laboratory equipment. The GSD process consists of exposing particular metals (Ni, Pd, Pt, Co), which act as ‘templates’, to a fuel rich combustion environment. As an exampl...

The cyclic voltammetry of red PbO, -PbO2, -PbO2 and BaPbO3 was studied with two different types of electrodes in acidic and alkaline media. In one case, microcrystalline particles of lead oxides were mechanically immobilized on the surface of paraffin-impregnated graphite rod electrodes (PIGE), while in the other case, lead oxides were added to a paste of graphite and silicone oil. The overall ...

Zuota is regarded as the king of Tibetan medicine. However, due to the confidentiality of this precious medicine, the scientific characterization of Zuota is very scarce, which limits the pharmacology and biosafety studies of Zuota. Herein, we collected four different Zuota samples from Tibet, Qinghai, Gansu, and Sichuan and characterized them by multiple techniques. Our results showed that Zuo...

This research work presents the study on fracture behavior of Al6061 with graphite particulate composite produced by the stir casting technique. The materials selected for the proposed work is Al6061 and graphite particles. Compact tension (CT) specimens were utilized to determine fracture toughness for different thickness of composite. In the present work, optimizing the parameters of the comp...

1. ABSTRACT X-ray diffraction (XRD) measurements have been made to determine residual stresses in embedded Al particles placed between the first and second ply of both unidirectional and fabric graphite/PMR-15 composite specimens. In order to further verify the results obtained, the effect of externally applied four-point bending on the measured strains and stresses in the Al inclusions was inv...