نتایج جستجو برای: calcinations

تعداد نتایج: 162  

2016
Naif Mohammed Al-Hada Elias Saion Zainal Abidin Talib Abdul Halim Shaari Frank Wiesbrock

Cadmium oxide semiconductor nanoparticles were produced using a water based mixture, incorporating cadmium nitrates, polyvinyl pyrrolidone (PVP), and calcination temperature. An X-ray diffraction (XRD) evaluation was conducted to determine the degree of crystallization of the semiconductor nanoparticles. In addition, scanning electron microscopy (SEM) was conducted to identify the morphological...

2013
Lakshmi M. Mukundan Remya Nirmal Dhanesh Vaikkath Prabha D. Nair

Bioactive glass is one of the widely used bone repair material due to its unique properties like osteoconductivity, osteoinductivity and biodegradability. In this study bioactive glass is prepared by the sol gel process and stabilized by a novel method that involves a solvent instead of the conventional calcinations process. This study represents the first attempt to use this method for the sta...

Journal: :Physical chemistry chemical physics : PCCP 2013
Junqing Yan Guangjun Wu Naijia Guan Landong Li Zhuoxin Li Xingzhong Cao

The sole effect of surface/bulk defects of TiO2 samples on their photocatalytic activity was investigated. Nano-sized anatase and rutile TiO2 were prepared by hydrothermal method and their surface/bulk defects were adjusted simply by calcination at different temperatures, i.e. 400-700 °C. High temperature calcinations induced the growth of crystalline sizes and a decrease in the surface areas, ...

Journal: :Journal of colloid and interface science 2014
Margarida Galhetas Ana S Mestre Moisés L Pinto Ibrahim Gulyurtlu Helena Lopes Ana P Carvalho

The high carbon contents and low toxicity levels of chars from coal and pine gasification provide an incentive to consider their use as precursors of porous carbons obtained by chemical activation with K2CO3. Given the chars characteristics, previous demineralization and thermal treatments were made, but no improvement on the solids properties was observed. The highest porosity development was ...

2012
P. C. Okonkwo

Lime production is a process that entail complex material and energy transport and chemical reaction. Efficient lime production processes are realized via well structured design models approach . Simulation of such process design models essentially provides Information on the attractive features and technical limitations of such processes which serves as guide for normal operations. The choice ...

2008
Sung-Chuan Lee

Synthesis of an inorganic molecularly imprinted polymer (MIP) composed of tetraethoxysilane (TEOS) for recognize sulfonamides using a sol-gel process have been developed. The template, sulfamethazine (SMZ), was dissolved in acid aqueous solution and added into TEOS to formed the precursor solution and adjusted the pH by various ammonium hydroxide (NH4OH) and reacted for 3 days. After the reacti...

Molecular sieves MCM-41 were synthesized from rice husk ash (RHA) as alternative sources of silica. The material was synthesized by a room temperature method from a gel with the molar composition SiO2: 1.6EA: 0.215HDTMABr: 325H2O with pH correction. The cetyltrimethylammonium bromide (CTMABr) was used as a structure template. Nanocomposite containing 5.0 and 10.0 wt.% of Cu was synthesized unde...

G. Mahmoudzadeh M. Zhalechin S. A. Khorrami S. S. Madani Sh. Moradi,

The aim of this study is to evaluate the influence of pH on the synthesis of nanocrystallines cobalt ferrite by combination of sol- gel auto combustion and ultrasonic irradiation methods. Two different fuels, urea and thiourea, along with metal nitrates (oxidant) were used to prepare CoFe2O4 powders. The morphology of the resulting powders was investigated. The powders wer...

Molecular sieves MCM-41 were synthesized from rice husk ash (RHA) as alternative sources of silica. The material was synthesized by a room temperature method from a gel with the molar composition SiO2: 1.6EA: 0.215HDTMABr: 325H2O with pH correction. The cetyltrimethylammonium bromide (CTMABr) was used as a structure template. Nanocomposite containing 5.0 and 10.0 wt.% of Cu was synthesized unde...

Mahsa Zarinkamar Majid Farahmandjou, Tahereh Pormirjafari Firoozabadi

Nano-crystalline particles of CeO2 have been synthesized by a low temperature chemical precipitation method. The precursor materials used in this research were Ce(NO3)3.6H2O, NaOH and diethylene glycol as surfactant. X-ray powder diffraction results showed that face centered cubic CeO2 nanoparticles with crystalline size in nanometer scale were formed. Scanning electron microscopy measurement s...

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