A simple, rapid, and sensitive method for the detection of posaconazole using dispersive liquid-liquid microextraction (DLLME) coupled to surface-assisted laser desorption/ionization mass spectrometric detection (SALDI/MS) was developed. After the DLLME, posaconazole was detected using SALDI/MS with colloidal gold and α-cyano-4-hydroxycinnamic acid (CHCA) as the co-matrix. Under optimal extract...

In this study, ultrasonic assisted machining (UAM) technique is applied in side-surface milling experiment for glass-ceramic workpiece material. The tungsten carbide cutting-tool with diamond coating is used in conjunction with two kinds of cooling/lubrication mediums such as water-soluble (WS) cutting fluid and minimum quantity lubricant (MQL). Full factorial process parameter combinations on ...

In this study, vibration cutting has been applied to machining of a novel material, NiTi based shape memory alloy (SMA), using a commercial ultrasonic piezoelectric transducer to vibrate an ISO insert CCMT geometry cutting tool. The effect of vibration in turning process was characterized by investigating the surface roughness of workpiece and surface quality assessment of machined surface usin...

For the first time, response surface methodology (RSM) using a Box-Behnken Design (BBD) was employed to optimize the conditions for ultrasonic assisted extraction (UAE) of antioxidants from Chinese sumac (Rhus typhina L.) fruits. Initially, influencing factors such as liquid-solid ratio, duration of ultrasonic assisted extraction, pH range, extraction temperature and ethanol concentration were ...

The process of ultrasonic-enhanced compound-enzymes-assisted extraction of polysaccharides from the fruit of Cornus officinalis was optimized by response surface methodology (RSM). The influence of three different factors on the yield of C. officinalis polysaccharides (COP) was studied. The results showed that the optimal conditions were extraction temperature 49.6 °C, ultrasound time 40.41 min...

Various extraction techniques were applied in the extraction of the biologically active constituents. The methods employed were traditional maceration extraction, microwave-assisted extraction(MAE), and ultrasound extraction (UE). Compared to the maceration extraction, MAE and UE methods provided high extraction yield, requiring short time frames and less labour. Microwave irradiation is a prov...

Ultrasonic-assisted plastic micro-forming is a research hotspot in metal-forming process. The friction characteristic key factor affecting the properties of metal ultrasonic-assisted However, existed researches were mostly focused on characteristics free surfaces, while few studied between sample and mold cavity. In this paper, micro double cup extrusion experiments copper T2 conducted to inves...

Mangiferin is a xanthone widely distributed in higher plants showing antioxidative, antiviral, anticancer, antidiabetic, immunomodulatory, hepatoprotective and analgesic effects. In the present study, an ultrasonic-assisted extraction method was developed for the effective extraction of mangiferin from mango leaves. Some parameters such as ethanol concentration, liquid-to-solid ratio, extractio...