نتایج جستجو برای: sol gel method and xrd technique

تعداد نتایج: 17121661  

2007
Ling-Sheng Jang Kuo-Ching Kuo

Lead Zirconate Titanate oxide (PZT) thick films with thicknesses of up to 10 μm were developed using a modified sol-gel technique. Usually, the film thickness is less than 1 μm by conventional sol-gel processing, while the electrical charge accumulation which reveals the direct effect of piezoelectricity is proportional to the film thickness and therefore restricted. Two approaches were adopted...

Journal: :Acta Crystallographica Section A Foundations of Crystallography 2008

M. Behpour, M. Mehrzad S. M. Hosseinpour-Mashkani

In this research, the thin films of N-S doped titanium dioxide (TiO2) were successfully prepared by simple sol-gel method in the presence of tetrabutylorthotitanate as a starting reagent. Furthermore, titanium dioxide (TiO2) was functionalized with thiourea. Furthermore, N-S doped titanium dioxides (NSTO) were fixed on glass balls by glass balls fixed-bed reactor system. Besides, the effect of ...

Journal: :international journal of nano dimension 0
z. shokri aghbolagh department of chemistry, payame noor university, abhar, zanjan, iran. a.r. mahjoub department of chemistry, faculty of science, tarbiat modares university, tehran, iran. sh. ghammamy department of chemistry, faculty of science, imam khomeini international university, qazvin, iran.

in this work, sol-gel processing was used to synthesize the fluorohydroxyapatite (nano-fha, ca10(po4)6(oh)2−xfx) nanopowders. the advantages of the sol-gel method over other methods are precise control of composition, low processing temperature, and better homogeneity. calcium nitrate tetrahydrate, phosphorous pentoxide and tetrabuthylammonium fluoride were used, respectively, as p, ca, and f p...

Journal: :Biomaterials 2001
M F Hsieh L H Perng T S Chin H G Perng

Calcium oxide was reported in the sol-gel-derived hydroxyapatite (HA) as an unavoidable major impurity. In this study phase purity of HA synthesized by sol-gel route was explored using precursors of calcium nitrate tetrahydrate and triethyl phosphate. Two different drying methods, the fast drying of as-prepared precursors and the slow drying of aged precursors were adopted as major processing v...

In this paper, indium tin oxide (ITO) nanoparticles has been prepared by chemical methods under given conditions with solution of indium chloride (InCl3·4H2O), tin chloride (SnCl4·5H2O) in ammonia solution. The samples were characterized by X-ray Diffraction (XRD) and scanning electron microscopy (SEM) analyses after heat treatments. The SEM results showed that, the size of the ITO particles pr...

In the current research project, sol-gel electrophoresis technique was utilized to grow titanium dioxide (TiO2) nanotubes. A titanium sol was prepared using organometallic precursors of titanium to fill the template channels. The prepared solwas driven into nanopores of porous anodic aluminum oxide templates under the influence of a DC electric field to form nanotubes on the pore walls. Tube fo...

Journal: :nanochemistry research 0
gunvant sonwane departmen of chemistry, kisan, arts, commerce and science college parola, dist-jalgaon, india. vilas mahajan departmen of chemistry, kisan, arts, commerce and science college parola, dist-jalgaon, india.

in this study, the ultrasonic, photocatalytic and sonophotocatalytic degradation of organics in textile industrial effluent was studied using zno nano catalyst, zno nano catalyst was synthesized by using sol-gel method. the structure and morphology of the catalyst were investigated using scanning election microscopy (sem), electron dispersive x-ray spectroscopy (eds) and x-ray diffraction patte...

Journal: :journal of ultrafine grained and nanostructured materials 2013
nasrin sasani heydar khadivi ayask seyed mojtaba zebarjad jalil vahdati khaki

high purity fluorapatite (fa) with rod-like and spherical-like morphology was synthesized via sol-gel method. chemical characterization of fa powders was done by xrd and ftir analyses. crystallite samples were calculated using scherer method. morphology of fa powders was investigated with tem and sem images. the results revealed that increasing the time of hydrolysis of phosphate sols significa...

2017
Mohamed Hassan Ahmed S. Afify Mohamed Ataalla Daniel Milanese Jean-Marc Tulliani

In this study, a glass ceramic with a nominal composition 58ZnO:4Bi₂O₃:4WO₃:33.3B₂O₃ was synthesized by melt quenching technique. A gas sensor was then manufactured using a ZnO sol-gel phase as a permanent binder of the glass-ceramic to an alumina substrate having interdigitated electrodes. The film sensitivity towards humidity, NH₃, H₂ and NO₂ was studied at different temperatures. X-ray diffr...

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