AbstractVarious nanoparticles have been investigated as novel drug delivery systems, including solid lipid nanoparticles (SLNs). Due to their rapid clearance from systemic circulation, nanoparticles do not provide sustained action in most cases. Different strategies have been employed to overcome this problem. In this direction, the present study introduces erodible in-situ forming gel systems ...

Hollow silica spheres with holes on the shells were prepared using l-16Ala6PyBr via a sol-gel method.

sol-gel and polymeric membrane electrodes, based on thiacalix[4]arene as a neutral carrier, weresuccessfully developed for the detection of vo2+ in aqueous solutions. the sol-gel and pvcmembrane electrodes exhibited linear response with nernstian slopes of 29.3 and 28.4 mv perdecade, respectively, within the vanadyl ion concentration ranges from 1.0 × 10-6 to 1.0 × 10-1mol dm-3 and from 1.0 × 1...

A glass-chip-based sample preparation method for matrix-assisted laser desorption/ionization mass spectrometric (MALDI-MS) analysis of tryptic digests of proteins and intact cells is described. A MALDI matrix, 2,5-dihydroxybenzoic acid (2,5-DHB), was hybridized with sol-gels to generate a sol-gel-derived material. Taking advantage of the characteristics of sol-gels, the sol-gel-derived material...

in this research zinc oxide (zno) nano-crystalline powders were prepared by sol-gel method using zinc acetate. the zno nanoparticles were characterized by x-ray diffraction (xrd), scanning electron microscopy (sem), ultraviolet-visible (uv-vis), fourier transform infra-red (ft-ir) and energy dispersive x-ray (edx) spectroscopy. the structure of nanoparticles was studied using xrd pattern. the c...

titanium dioxide nanocrystals were synthesized by sol-gel method at room temperature. titanium isoprophoxide and absolute ethanol were used as precursors to prepare the sol. the ph of the solution was adjusted by adding nitric acid and sodium hydroxide solution. the prepared tio2 nanocrystals were annealed at 325°c, 425°c and 525°c respectively. the effect of ph on the surface morphology and st...

Recent developments in the preparation of surfactant-templated mesostructured sol-gel silica materials have extended the morphology from the originally discovered powders, with particle sizes on the order of microns, to mesoporous continuous thin films. These films could find applications in membrane-based separations, selective catalysis and sensors. Particularly, sodium dodecyl sulfate (SDS)t...

zno thin films with preferred orientation along the (002) plane were prepared onto the glass substrates by the sol-gel spin coating method for different post- annealing temperatures. the xrd study confirms that the thin films grown by this method have good crystalline hexagonal wurtzite structure. the optical band gap of the samples was determined from uv-visible spectra. it is found that the s...

this article describes the preparation and analysis of nano hydroxyapatite (ha) films on stainless steel 316l through sol-gel technique. the process started with preparation of a nitrate and phosphate sol. after aging the sol for 24 h at room temperature a ss316 substrate was dip-coated and heat-treated at 350 to 450 °c for different times in air. the coating phase and structure on substrate we...

in this paper, labo3 perovskite type catalyst formulations were prepared by sol-gel auto combustion method using citric acid as the fuel. activity of catalysts was tested in catalytic oxidation of toluene as a model of volatile organic compounds. lacoo3 perovskite formulation showed the highest activity among labo3 (fe, mn and co) perovskite catalysts. so, lacoo3 perovskite based catalyst was s...