نتایج جستجو برای: sol gel auto combustion method
تعداد نتایج: 1769607 فیلتر نتایج به سال:
Nanocrystalline Li0.35Ni0.3Fe2.35O4 ferrites were prepared at different annealing temperatures by sol–gel auto-combustion method. The effects of the temperature on structure and magnetic properties synthesized Li–Ni characterized X-ray diffraction (XRD), scanning electron microscopy, Fourier transform infrared spectra Vibrating Sample Magnetometer, photoelectron spectrometer. Rietveld refinemen...
Abstract: Auto-ignited gel combustion process has been used for producing a red hematite-zircon based pigment. The combustible mixtures contained the metal nitrates and citric acid as oxidizers and fuel, respectively. Sodium silicate (water glass) was used as silica source for producing zircon phase. X-Ray Diffractometery, Electron Microscopy and Simultaneous Thermal Analysis were used for ...
This work focuses on the microstructure, magnetic properties and magnetocaloric effect of CoFe$_2$O$_4$ (CFO) nanoparticles elaborated by sol-gel auto combustion method. The XRD investigation indicates that CFO is crystallized in a cubic spinel structure SEM micrograph shows fine quasi-spherical with an average grain sizes 160 nm. temperature dependence Raman spectra reveals ferromagnetic to pa...
In this research, NTC thermistors with composition of NiMn2-xCoxO4 (x = 0.4, 0.8, 1.2, 1.6) prepared by two methods: solid state reaction and sol-gel (gel-combustion). The average particle size was monitored and structure of the calcinated powders have been investigated using x-ray diffraction (XRD) and tunneling electron microscopy (TEM) techniques. The average particle size was estimated to b...
The aim of this study is to evaluate the influence of pH on the synthesis of nanocrystallines cobalt ferrite by combination of sol- gel auto combustion and ultrasonic irradiation methods. Two different fuels, urea and thiourea, along with metal nitrates (oxidant) were used to prepare CoFe2O4 powders. The morphology of the resulting powders was investigated. The powders wer...
the mössbauer spectra of nanoferrite materials such as ni0.25mn0.75fe2o4, co0.5mn0.5fe2o4 and ni0.4co0.6fe2o4 have been reported and the above materials were prepared by sol-gel combustion method using metal nitrates as source material and polyvinyl alcohol(pva) as agglomeration reducing agent. as the structural, thermal and magnetic properties (vsm) of the above ferrites have been published al...
trontium hexaferrite (SrFe 12 O 19 ) nanosized powders were synthesized by sol-gel auto-combustion method with and without cetyltrimethylammonium boromide (CTAB) addition in the sol with Fe/Sr ratio of 11 (using additional Sr). The resultant powders were investigated by X-ray Diffraction (XRD), Transmission Electron Microscope (TEM), Field Emission Scanning Electron Microscope (FESE...
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