An aberration-corrected JEOL 2200FS scanning-transmission electron microscope (STEM), equipped with a high-angle annular dark-field detector (HAADF), is used to monitor the coalescence and sintering of Pt nanoparticles with an average diameter of 2.8 nm. This in situ STEM capability is combined with an analysis methodology that together allows direct measurements of mass transport phenomena tha...

Recent research has been significantly increased our fundamental understanding of microwave interactions with materials. Thermal absorption has been demonstrated to result from simultaneous action of multiple dissipation mechanisms during processing. In addition, it has been conclusively established that strong microwave fields exert a non-thermal driving force during sintering. This force acts...

The aim of the present investigation was to formulate thermally sintered floating tablets of propranolol HCl, and to study the effect of sintering conditions on drug release, as well as their in vitro buoyancy properties. A hydrophilic polymer, polyethylene oxide, was selected as a sintered polymer to retard the drug release. The formulations were prepared by a direct compression method and wer...

Microwave processing is emerging as an innovative and highly effective material processing method offering many advantages over conventional methods, especially for sintering applications. It is recognized for its various advantages, such as: time and energy saving, rapid heating rates, considerably reduced processing cycle time and temperature, fine microstructures and improved mechanical prop...

Bioglass® 45S5 is widely used in biomedical applications due to its ability to bond to bone and even to soft tissues. The sintering ability of Bioglass powders is a key factor from a technological point of view, since its govern the production of advanced devices, ranging from highly porous scaffolds to functionalized coatings. Unfortunately this particular glass composition is prone to crystal...

The room-temperature magnetic properties of ball-milled strontium hexaferrite particles consolidated by spark-plasma sintering are strongly influenced by the milling time. Scanning electron microscopy revealed the ball-milled SrFe12O19 particles to have sizes varying over several hundred nanometers. X-Ray powder-diffraction studies performed on the ball-milled particles before sintering clearly...

the fabrication of complex-shaped parts out of (wt %) co-28cr-6mo alloy by three-dimensional printing (3dp) was studied using two grades of the alloy with average particle sizes of 20 and 75 μm. to produce sound specimens, 3dp processing parameters were tuned. the sintering behavior of the powders was characterized by the dilatometric analysis. batch sintering in argon atmosphere at 1280 °c for...

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Fabrication of mechanically competent bioactive scaffolds is a great challenge in bone tissue engineering. In this paper, β-tricalcium phosphate (β-TCP) scaffolds were successfully fabricated by selective laser sintering combined with furnace sintering. Bioglass 45S5 was introduced in the process as liquid phase in order to improve the mechanical and biological properties. The results showed th...