Due to the complex nature of the proteome, instrumentation and methods development for sample cleanup, fractionation, preconcentration, chromatographic separation and detection becomes urgent for the identification of peptides and proteins. Newly developed techniques and equipment for separation and detection, such as nanoHPLC and multidimensional HPLC for protein and peptide separation, enable...

N. Burham; S.M.Abdel-Azeem; M. F. El-Shahat, Separation and determination of trace amounts of zinc, lead, cadmium and mercury in tap and qaroun lake water using polyurethane foam functionalized with 4-hydroxytoluene and 4-hydroxyacetophenone,Analytica Chimica Acta 579 (2006) 193–201. Abstract : N. Burham; S.M.Abdel-Azeem; M. F. El-Shahat, Determination of lead and cadmium in tap water and apple...

Due to the complex nature of the proteome, instrumentation and methods development for sample cleanup, fractionation, preconcentration, chromatographic separation and detection becomes urgent for the identification of peptides and proteins. Newly developed techniques and equipment for separation and detection, such as nano-HPLC and multidimensional HPLC for protein and peptide separation, enabl...

The aim of this article is to review the recent progress in coupling membrane separation and electrochemical technologies for water treatment. Process integration strategies have been classified three groups. first group deals with electrocoagulation electrooxidation as pretreatment separation, most cases aimed at reducing fouling decay permeate flux porous ultrafiltration membranes. second ded...

Recently, coal fly ash has become a potential candidate as secondary resource of rare earth elements (REE). In this investigation, we studied the recovery REE from commercial power plant. The specific aim was to assess technical feasibility recovering using conventional preconcentration methods, including gravity separation, magnetic and froth flotation. experimental results revealed that flota...

A magnetic nano-composite based on modified styren-maleic anhydride copolymer and Fe3O4 nano-particles was introduced as a new sorbent for solid-phase extraction and preconcentration of trace levels of silver ion from aqueous solutions. The size and morphology of the nano-sorbent were characterized via X-ray diffraction analysis, scanning electron microscopy and Fourier transform infrared spect...

A microchip electrospray emitter with a magnetic bead trap has been designed for solid-phase extraction-gradient elution-mass spectrometry (SPE-GEMS). The goal of this method is the detection of analytes at low concentrations and it is here demonstrated using reverse phase coated magnetic beads (Mbs) for the preconcentration and detection of the peptides. The sample is passed through the chip, ...

Different source preparation procedures for determination of uranium radioisotopes in environmental samples by alpha spectrometry are presented. Addition 232 U tracer was followed the preconcentration radionuclides interest from co-precipitation on Fe(OH) 3 at pH 9 using ammonia solution. The extracts were obtained column separation UTEVA resin after which sources prepared either electrodeposit...

An efficient and simple magnetic solid phase extraction based on the use of CoFe3O4 nanoparticles grafted multi-walled carbon nanotubes (MWCNTs) as adsorbent coupled with surfactant enhanced spectrofluorimetric detection...