Reduction of an oxide in hydrogen is a method frequently employed in the preparation of active catalysts and electronic devices. Synchrotron-based time-resolved X-ray diffraction (XRD), X-ray absorption fine structure (NEXAFS/EXAFS), photoemission, and first-principles density-functional (DF) slab calculations were used to study the reaction of H(2) with nickel oxide. In experiments with a NiO(...

Bismuth oxide directly grown on nickel foam (p-Bi2O3/Ni) was prepared by a facile polymer-assisted solution approach and was used directly as a lithium-ion battery anode for the first time. The Bi2O3 particles were covered with thin carbon layers, forming network-like sheets on the surface of the Ni foam. The binder-free p-Bi2O3/Ni shows superior electrochemical properties with a capacity of 66...

The synthesis of NiO nanoparticles was done by sol-gel method. Nickel Acetate Tetrahydrate ((CH3COO)2 –Ni·4H2O) was dissolved in ethanol with constant stirring to obtain a clear and light greenish sol. Oxalic acid solution was used to obtain a thick green gel, then dried in an oven to get dried gel and was then grinded into fine powders and calcined for different time periods to obtain nanocrys...

–The use of powder of calcined brick (PCB) as the low-cost adsorbents was investigated as a replacement for current costly methods of removing nickel ions from aqueous solutions. Batch adsorption studies were conducted to examine the effects of physico-chemical key parameters such as the stirring rate, initial metal ion concentration, pH, agitation time, particle size and adsorbent dosage on th...

In this work, the following studies were carried out: structure of starting materials (metal‑powder composition) heat‑resistant nickel alloys EP648 and VJ159; sphericity, fluidity bulk density powder particles from elemental (chemical) composition effect technological energy parameters laser radiation on defect formation (pore) in manufactured (grown) blanks (samples); samples VJ159. Based resu...

In the present work, six-layered (Zirconia/Nickel) functionally graded materials were fabricated via powder metallurgy technique (PMT). The microstructure, fracture surface and the elemental analysis of the prepared components were studied, and their linear shrinkage, electrical conductivity, fracture toughness and Vickers hardness were evaluated. The results show that the linear shrinkage of t...

Ni6(N2H4)6(SO4)4(OH)2(H2O)8](SO4)(H2O)10 complex was prepared according to literature report. The reaction between aforementioned complex via sodium alkoxides as a reactants, were carried out in the solid state. The [Ni6(N2H4)6(SO4)4(OH)2(H2O)8](SO4)(H2O)10 undergoes an intramolecular two electrons oxidation-reduction reaction at room temperature and metallic nickel nanoparticles (Ni1-Ni5) was ...

Abstract: activity gas diffusion process has been investigated in this research. Effects of coating temperature and aluminumconcentration in powder mixture on formation mechanism were studied using optical and scanning electronmicroscopes, EDS and X-ray diffraction (XRD) techniques. For this purpose two different packs containing 1 and 2wt% aluminum powder, were used for coating the samples at ...