Nanoparticles of a one-dimensional coordination polymer [Pb(L)(μ2-I)]n (1), (Lˉ = 1H1,2,4-triazole-3-carboxylate), have been synthesized by a sonochemical process and characterized by field emission scanning electron microscopy (FESEM), X-ray powder diffraction (XRPD), FT-IR spectroscopy and elemental analyses. The thermal stability of compound 1 both its bulk and nano-size has been studied by ...

Nano-zeolite CoAPO-5 as a member of AFI family, was synthesized via a hydrothermal treatment, and structurally characterized using X-ray diffraction (XRD), scanning electron microscope (SEM), and energy dispersive X-ray analysis (EDAX). The effects of crystallization temperature and time on the structure of these powder products were studied. XRD patterns of the synthesized powders revealed a h...

The densification response of aluminium powder reinforced with nanometric SiC particles (50 nm) during uniaxial compaction was studied. To determine the effect of SiC nanoparticles on the compressibility of the matrix, monolithic Al powder was also examined. The effect of SiC nanoparticles on the densification mechanisms, i.e. particle rearrangement and plastic deformation, was analysed using m...

This paper provides an overview on our recent investigations on the consolidation of hierarchy-structured nanopowder agglomerates and related applications to net-shaping nanopowder materials. Understanding the nanopowder agglomerate sintering (NAS) process is essential to processing of net-shaped nanopowder materials and components with small and complex shape. The key concept of the NAS proces...

The research investigates synthesized Nano-structured PbO2 using ball milling. The structure and morphology of the samples were determined in the process of milling by means of XRD and SEM. The size of particles was estimated through DLS analysis. The TEM image of the synthesized powder verifies the achievement of Nano dimensions. Design and analyses of the results using Taguchi methodology rev...