نتایج جستجو برای: modified solid state route

تعداد نتایج: 1294359  

Journal: :Molecules 2017
Kenta Nishino Kyoya Uemura Masayuki Gon Kazuo Tanaka Yoshiki Chujo

The enhancement of aggregation-induced emission (AIE) is presented on the basis of the strategy for improving solid-state luminescence by employing multiple o-carborane substituents. We synthesized the modified triphenylamines with various numbers of o-carborane units and compared their optical properties. From the optical measurements, the emission bands from the twisted intramolecular charge ...

ZnO/activated carbon nanocomposites (ZnO/ACns) were synthesized by applying two different solid-state and precipitation methods. Precipitation method was initiated with zinc chloride and sodium hydroxide as starting materials in the presence of activated carbon. The synthesized sample was calcined at 250 °C for 1 h. The preparation of nanocomposite by solid-state method was accomplished by heat...

N.sitophila was grown under controlled conditions of solid state and submerged fermentation on Sago hampas. The optimum conditions of protein enrichment previously established for sugar beet pulp was used for this study. Under this condition the protein content of Sago hampas under solid state increased from 1.4 to 14.45% (W/W) whereas for Sago hampas and Sago starch, the protein content under ...

Journal: :Organic & biomolecular chemistry 2013
David Parker Bradley P Waldron

Synthetic approaches are reported to polydentate ligands based on 6-phenyl-6-amino-perhydro-1,4-diazepine. The synthetic route devised averts ring-opening reactions, allowing the exocyclic N-substituent to be introduced separately and involves a nitro-Mannich condensation, prior to chemoselective RANEY® nickel reduction. Comparison of the solid-state structures of four synthetic intermediates r...

2015
Jie Ding Zhennan Huang Jihao Zhu Shengzhong Kou Xiaobin Zhang Hangsheng Yang

High-ordered anatase TiO2 nanotube array films coated with exposed high-reactive {001} nanofacets were fabricated by a modified hydrothermal method using amorphous anodic TiO2 nanotube arrays (ATONAs) as starting materials. It was found that the reaction between gas phase HF and solid ATONAs played a key role in the transformation process from amorphous to anatase TiO2, and the TiO2 tubular str...

Gitika Arorac Harish Durejab Manju Nagpal, Pankaj Rakha Surender Goyal Veerendra Rajpurohit

      In order to enhance in vitro dissolution and content uniformity of poorly soluble drug glimepiride by preparing solid dispersions using modified solvent fusion method, solid dispersions of drug were prepared by modified fusion solvent method using PEG 6000 and PVP K25 (as carrier). Eight batches (F1-F8) were prepared by Factorial design (23) by taking three ...

2014
Gaurav Bhatia Vivek Kumar

Traditional TCP cannot detect link contention losses and route failure losses which occur in MANET and considers every packet loss as congestion. This results in severe degradation of TCP performance. In this research work, we modified the operations of TCP to adapt to network states. The cross-layer notifications are used for adapting the congestion window and achieving better performance. We ...

Journal: :Ceramics International 2021

Bismuth titanate is a lead-free piezoelectric ceramic with outstanding properties that strictly depend on the composition and microstructure. However, bismuth-based materials are difficult to synthesize due bismuth volatilisation causes secondary phases stoichiometry deviations. In this work, we propose low-temperature chemical route, i.e. modified amorphous citrate method, allows reduction of ...

2013
Hailong Wang Luis A. Zepeda-Ruiz George H. Gilmer Moneesh Upmanyu

Vapour-liquid-solid route and its variants are routinely used for scalable synthesis of semiconducting nanowires, yet the fundamental growth processes remain unknown. Here we employ atomic-scale computations based on model potentials to study the stability and growth of gold-catalysed silicon nanowires. Equilibrium studies uncover segregation at the solid-like surface of the catalyst particle, ...

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