نتایج جستجو برای: epimerization

تعداد نتایج: 549  

Journal: :Organic & biomolecular chemistry 2009
Taku Yoshiya Hiroyuki Kawashima Youhei Sohma Tooru Kimura Yoshiaki Kiso

We report the establishment of the O-acyl isopeptide method-based racemization-free segment condensation reaction toward future chemical protein synthesis. Peptide segments containing C-terminal O-acyl Ser/Thr residues were successfully synthesized by use of a lower nucleophilic base cocktail for Fmoc removal, and then coupled to an amino group of a peptide-resin without side reactions or epime...

Journal: :Angewandte Chemie 2015
Chenlong Zhu Zhaobo Liu Guanyu Chen Kai Zhang Hanfeng Ding

A concise total synthesis of rac-alsmaphorazine D has been described for the first time. The efficient synthetic strategy features four key transformations: 1) a catalytic intramolecular oxidative cyclization for the δ-lactamindole backbone; 2) an oxidative cyclic aminal formation for the hexahydropyrrolo[2,3-b]pyrrole framework; 3) a transannular radical cyclization for the construction of the...

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