Using examples from various domains of science, this review covers some recent developments in spectrum imaging (SI) using scanning transmission electron microscopy (STEM) and electron energy loss spectroscopy (EELS). Advanced multi-dimensional acquisition methods allow the acquisition of STEM-EELS data with other complementary data such as energy dispersive X-ray spectroscopy (EDS), cathodolum...

The microstructure and micro-composition of ZnO thin films doped with Al, deposited on Si/SiO2 substrates by sol-gel method were investigated by scanning and high resolution transmission electron microscopy and related energy dispersive X-ray analyses (SEM-EDX, STEM-HRTEM/EDX). Thin films of ZnO were prepared by deposition of 1-10 successive layers with 0.5 at.% and 5 at.% Al concentrations. Th...

We demonstrated a facile and environmental-friendly approach to form gold nanoparticles through the reduction of HAuCl4 by aspartame. The single-crystalline structure was illustrated by transmission electron microscopy (TEM) and X-ray diffraction (XRD). The energy-dispersive X-ray spectroscopy (EDS) and Fourier transform infrared (FTIR) results indicated that aspartame played a pivotal role in ...

The use of closed, electron transparent gas cells to perform in situ scanning/ transmission electron microscopy (S/TEM) now enables visualization of the atomic structure of catalysts at variable temperature in a gas environment, which may be close to real operational conditions [1]. When coupled with energy dispersive spectroscopy (EDS) detector, in situ composition analysis can be achieved at ...

Since the first demonstration of atomically resolved energy dispersive x-ray spectroscopy (EDX) using a scanning transmission electron microscope (STEM) in 2010 [1], theory based simulations established that EDS hyperspectral maps could be used to measure atomic distances. That is, EDX is an incoherent imaging mode and signal intensity corresponds directly to the structure of the sample [1]. It...

In this work we describe thickness measurements from oxide layers on uranium and tantalum using Energy Dispersive Spectroscopy (EDS) combined with Oxford Instruments software calculating the layer thickness from measured X-ray intensities. A comparison of the oxide distribution is shown between (1) a user standardised system with an older SDD detector and INCA ThinFilmID and (2) the latest larg...

In this work, Sn-Cu composite powders were produced using an electroless process. The tin content on the surface of copper powders was varied by using di erent concentrations of SnSO4 in the plating bath. The surface morphology of the produced Sn-Cu composite powders was characterized using scanning electron microscopy (SEM). Energy dispersive spectroscopy (EDS) was used to determine the elemen...

An anisotropic conductive adhesive (ACA) bump was produced on a silicon chip for bonding onto a glass substrate. The bumping process and the bonding procedure are described. The constituents of the ACA were investigated with a scanning electron microscope (SEM) and energy dispersive spectroscopy (EDS). The thermal behavior of the ACA was investigated with differential scanning calorimetry (DSC)...

The feasibility of utilizing disordered Ni-based metal hydroxide, as both the anode and the cathode materials, in alkaline rechargeable batteries was validated for the first time. Co and Mn were introduced into the hexagonal Ni(OH)2 crystal structure to create disorder and defects that resulted in a conductivity increase. The highest discharge capacity of 55.6 mAh ̈g ́1 was obtained using a comme...

The first laboratory synthesis of hard materials such as diamond proceeded to attack of developing materials with high hardness to compete diamond. Boron rich solids are good candidates owing to their short interatomic bond lengths and strong covalent character. Boron containing hard material was synthesized by modifiedmicrowave method under nitrogen atmosphere by using a fuel (glycine or urea)...