The asymmetric unit of title hydrated salt, C22H46N4 (2+)·2Cl(-)·4H2O, comprises half a centrosymmetric dication, one Cl(-) anion and two water mol-ecules of crystallization. The structure determination reveals that protonation has occurred at diagonally opposite amine N atoms, and that the dication features intra-molecular N-H⋯N hydrogen bonds. In the crystal, a three-dimensional artchitecture...

Procedures for the isolation, purification, and crystallization of wheat germ agglutinin are described. The agglutinin was purified 184-fold to homogeneity from commercial wheat germ lipase. A molecular weight of 23,500 was estimated for the protein by means of sedimentation equilibrium and sodium dodecyl sulfate gel electrophoresis. The agghxtinin is a glycoprotein. Amino acid and carbohydrate...

perlite or pearl stone is a natural glass which has formed by rapid cooling of viscous lava or magma. perlite is mainly composed of silica, aluminum, potassium and sodium. in this experiment, perlite was used as a low-cost source of si and al to synthesis of sodalite zeolite using the alkaline hydrothermal treatment. a statistical taguchi design of experiments was employed to evaluate the effec...

Nano-zeolite CoAPO-5 as a member of AFI family, was synthesized via a hydrothermal treatment, and structurally characterized using X-ray diffraction (XRD), scanning electron microscope (SEM), and energy dispersive X-ray analysis (EDAX). The effects of crystallization temperature and time on the structure of these powder products were studied. XRD patterns of the synthesized powders revealed a h...

Thin films of GeTe2 were deposited on glass substrates using radio-frequency magnetron sputtering with various hydrogen flow rates in the growth chamber. Transmission data of deposited films were taken and used to determine optical constants refractive index n , extinction coefficient , and absorption coefficient and the energies corresponding to absorption coefficients of 104 and 103 cm−1 E04,...

We have found that treatment of the photosynthetic membranes of green plants, or thylakoids, with the nonionic detergent Triton X-114 at a 10:1 ratio has three effects: (a) photosystem I and coupling factor are solubilized, so that the membranes retain only photosystem II (PS II) and its associated light-harvesting apparatus (LHC-II); (b) LHC-II is crystallized, and so is removed from its norma...

Laser Powder Bed Fusion (LPBF) of thermoplastic polymers is an additive manufacturing (AM) technique experiencing a remarkable growth in the recent years. Nowadays most widely used materials are polyamides (PA12, PA11…) but massively available LPBF-compatible polyolefin powders recently arrived on market. The need understanding crystallization process for these new essential and this was addres...

By using the seeding technique the nucleation rate for the formation of ice at room pressure will be estimated for the TIP4P/ICE model using longer runs and a smaller grid of temperatures than in the previous work. The growth rate of ice will be determined for TIP4P/ICE and for the mW model of water. Although TIP4P/ICE and mW have a similar melting point and melting enthalpy, they differ signif...

In 1986, Kawashima and their coworkers developed the spherical crystallization technique for size enlargement of the drug in the field of pharmacy. Kawashima defined spherical crystallization as “An agglomeration process that transforms crystals directly into compact spherical forms during the crystallization process.” It also enables co-precipitation of drug and encapsulating polymer in the fo...