SYNLETT 2004, No. 6, pp 1054–105806.05.2004 Advanced online publication: 25.03.2004 DOI: 10.1055/s-2004-822895; Art ID: G04404ST © Georg Thieme Verlag Stuttgart · New York Abstract: Using only 10% of CrCl2 as catalyst, manganese-powder as reducing agent and TMSCl as scavenger, 2-methylene-a,w-dialdehydes and -ketones can be coupled to form cyclic diols diastereoselectively. The diastereomeric e...

Nonlinear Compton scattering has been observed in the collision of a low-emittance 46.6-GeV electron beam with terawatt pulses from a Nd:glass laser at 1054 and 527 nm wavelengths in an experiment at the Final Focus Test Beam at SLAC. Peak laser intensities of 1018 Wycm2 have been achieved, corresponding to a value of 0.6 for the parameter h ­ eErmsymv0c. Results are presented for multiphoton C...

The present study extends the range of flow patterns observed during boiling of water in a single minichannel of height 197 μm and width 1054 μm. The calculated hydraulic diameter of the channel is 333 μm. High-speed photography is used to obtain video images of the flow field. The top covers of the channels are made of Lexan to permit visual observation, while the minichannel is machined in a ...

n engl j med 365;11 nejm.org september 15, 2011 1054 4. Freeman JV, Zhu RP, Owens DK, et al. Cost-effectiveness of dabigatran compared with warfarin for stroke prevention in atrial fibrillation. Ann Intern Med 2011;154:1-11. 5. Ruff CT, Giugliano RP, Antman EM, et al. Evaluation of the novel factor Xa inhibitor edoxaban compared with warfarin in patients with atrial fibrillation: design and rat...

2014 The scattering factor of polyelectrolyte solutions in the absence of added salt presents a peak at a scattering vector qm which varies like C 1/2. This has been sometimes interpreted in terms of a local orientational order of cylinders. The variation holds however through many concentration regimes, and other explanations in term of correlation holes have been proposed. We evaluate the dif...

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Threshold phenomena are investigated using a general approach, following Talagrand [Ann. Probab. 22 (1994) 1576–1587] and Friedgut and Kalai [Proc. Amer. Math. Soc. 12 (1999) 1017–1054]. The general upper bound for the threshold width of symmetric monotone properties is improved. This follows from a new lower bound on the maximal influence of a variable on a Boolean function. The method of proo...

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Circulation. 2016;134:1054–1056. DOI: 10.1161/CIRCULATIONAHA.116.024043 ECG ChallEnGE A 21-year-old woman without prior cardiac history presented to the emergency department with palpitations. On telemetry she was noted to have a paroxysmal supraventricular tachycardia with no discernible P waves. She was given 6 mg of intravenous adenosine with prompt conversion to normal sinus rhythm. Thirty ...