Masoud Ghanei-Motlagh

Sirjan Branch, Islamic Azad University

[ 1 ] - Construction of a Carbon Paste Electrode Based on Novel Thiolated Ligand Capped Gold Nanoparticles for Determination of Trace Amounts of Mercury(II)

In the present study, a simple electrochemical sensor for trace determination of Hg(II) ions in aqueous solutions was introduced. The proposed sensor was designed by incorporation of the 4-methyl-piperidine-carbodithioate capped gold nanoparticles (GNPs) into the carbon paste electrode (CPE), which provides a remarkably improved sensitivity for stripping voltammetric determination of Hg(II). Di...

[ 2 ] - Synthesis and Application of Novel Modified Magnetic Nanocomposite for Solid Phase Extraction of Thallium(I) Ions

In this paper, magnetically multiwalled carbon nanotubes (MMWCNTs) nanocomposite modified by methyl-2-[2-(2-2-[2-(methoxycarbonyl) phenoxy] ethoxyethoxy) ethoxy] benzoate was applied for magnetic solid-phase extraction (MSPE) of thallium(I) ions. Fourier transform infrared (FT-IR) spectroscopy, field emission scanning electron microscopy (FE-SEM), X-ray diffraction (XRD) spectrometry and vibrat...

[ 3 ] - An Electrochemical Sensor Based on Novel Ion Imprinted Polymeric Nanoparticles for Selective Detection of Lead Ions

In this study, the novel surface ion-imprinted polymer (IIP) particles were prepared and applied as a electrode modifier in stripping voltammetric detection of lead(II) ion. A carbon paste electrode (CPE) modified with IIP nanoparticles and multi-walled carbon nanotubes (MWCNTs) was used for accumulation of toxic lead ions. Various factors that govern on electrochemical signals including carbon...

[ 4 ] - Determination of Rhodium(III) Ions by Flame Atomic Absorption Spectrometry after Preconcentration with Modified Magnetic Activated Carbon

A new method for analysis of trace amount of Rh(III) ions by magnetic activated carbon modified with 2,3,5,6-tetra(2-pyridyl)pyrazine (MAC/TPPZ) as the magnetic sorbent has been proposed. The proposed adsorbent was found to be advantageous over conventional solid phase extraction (SPE) in terms of operational simplicity and low time-consuming. The experimental parameters affecting the extractio...

[ 5 ] - Application of Sulfur Nanoparticles as a Solid Phase Extraction Sorbent for the Preconcentration of Lead(II) and Palladium(II) in Environmental Samples Prior to Flame Atomic Absorption Spectrometry Determination

The application of sulfur nanoparticles as an efficient adsorbent for the solid-phase extraction and determination of the trace amounts of Pb and Pd ions was investigated in environmental samples using flame atomic absorption spectrometry. Effects of various parameters such as pH, flow rate of sample and eluent, type and concentration of eluent, sample volume, amount of adsorbent and interferin...