Preparation and Characterization of ZrO2/ZnO Nanocomposite under Ultrasonic Irradiation via Sol-gel Route

Authors

  • A. Farhadyar Agribusiness Department, Armenian State Agrarian University, IRAN
  • M. Zare-Dehnavi Department of Chemistry, East Tehran Branch, Islamic Azad University, Tehran, Iran
  • N. Farhadyar Department of Chemistry, Varamin-Pishva Branch, Islamic Azad University, Varamin, Iran
  • Sh. Aghabeygi Department of Chemistry, East Tehran Branch, Islamic Azad University, Tehran, Iran
Abstract:

Nanocomposite of ZrO2/ZnO was prepared under ultrasonic irradiation by sol gel process from directly mixing Zirconium and Zinc gels, and the mixture was placed under ultrasonic irradiation for 2 hours then aging time the filtrated composite gel was calcinated at 500°C for 3h in furnace. The precursor sol of zirconium was prepared from an aqueous solution of ZrCl4 and zinc acetate dihydrated was dissolved in de-ionized water. The FT-IR analysis and the XRD study were exhibited that the crystal structure and purity of the ZrO2/ZnO nanocomposite FESEM images was indicated the morphology and the average size of the NPs. The average size of the ZrO2/ZnO nanocomposite was determined 37 nm.

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Journal title

volume 4  issue 1

pages  35- 38

publication date 2015-04-01

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