Lactic-based Novel Amine Ionic Liquid: Synthesis and Characterization of [DEA][Lac]

Authors

  • Ali Hojatnia Department of Chemical Engineering, Faculty of Energy, Kermanshah University of Technology, Kermanshah, Iran
  • Mohsen Samimi Department of Chemical Engineering, Faculty of Energy, Kermanshah University of Technology, Kermanshah, Iran
Abstract:

In this study, a novel amine ionic liquid “Diethanolamine Lactic” [DEA][Lac] was synthesized. The replacement of halogenated ion fluid was used as a modified methodology for the preparation of diethanolamine based on lactic acid. The ionic liquid was characterized using the Fourier transform infrared (FTIR) spectra and the nuclear magnetic resonance (NMR) spectroscopy. The changes in bands' wavelengths and the peaks of the participating elements and process materials have been confirmed before and after synthesis based on the results of FTIR analysis which demonstrate the successful synthesis of diethanolamine lactic. The NMR analysis also clearly confirms the synthesis of diethanolamine lactic acid. Analysis results were shown in the successful synthesis of the [diethanolamine] [lactic].   

Upgrade to premium to download articles

Sign up to access the full text

Already have an account?login

similar resources

synthesis and characterization of some macrocyclic schiff bases

ماکروسیکلهای شیف باز از اهمیت زیادی در شیمی آلی و دارویی برخوردار می باشند. این ماکروسیکلها با دارابودن گروه های مناسب در مکانهای مناسب می توانند فلزاتی مثل مس، نیکل و ... را در حفره های خود به دام انداخته، کمپلکسهای پایدار تولید نمایند. در این پایان نامه ابتدا یک دی آلدئید آروماتیک از گلیسیرین تهیه می شود و در مرحله بعدی واکنش با دی آمینهای آروماتیک و یا آلیفاتیک در رقتهای بسیار زیاد منجر به ت...

15 صفحه اول

Ionic liquid-assisted synthesis, characterization and photocatalytic properties of SnO microflowers with nanosheet subunits

In this study, simple ionic liquid-assisted preparation of SnO microflowers with nanosheet subunitsunder reflux condition without calcination were described. Samples were synthesized using 1-pentyl-3-methylimidazolium bromide, [pmim]Br, as an ionic liquid in different molar ratio, sodium hydroxideand Tin(II) chloride. The results show that SnO with high purity and uniform size...

full text

synthesis and characterization of potentially biological active cyclometallated organoplatinum(ii) complexes

this work is presented in five parts. in the first part preparation of the starting complex [pt(c^n)cl(dmso)], 1, in which c^n = n(1),c(2?)-chelated, deprotonated 2-phenylpyridine, and dmso = dimethylsulfoxide, and its reaction with 1 equiv of the biphosphine ligands bis(diphenylphosphino)amine, dppa, or bis(diphenylphosphino)methane, dppm, to give the complex [pt(c^n)cl(dppa)], 2, or [pt(c^n)c...

15 صفحه اول

synthesis and characterization of some new cyclometalated organoplatinum(ii) complexes containing phosphite ligand

در این تحقیق روشی جهت سنتز یک سری از کمپلکس های پلاتین (ii) حاوی لیگاند های دهنده ی فسفری شامل فسفیت و فسفین ارائه شده است. واکنش پیش ماده ی پلاتین (ii)،trans/cis- [ptcl2(sme2)2] ، با 2 اکی مولار از لیگاند p(oph)3در حلال بنزن کمپلکس1، cis-[ptcl2(p(oph)3)2] را تولید می نماید. جهت سنتز کمپلکس سایکلو متال فسفیتی، کمپلکس 1 با 1 اکی والان واکنشگر ptcl2 در حلال زایلن در شرایط رفلاکس زیر گاز آرگون م...

Synthesis and Characterization of Novel Nanodiopsidebioceramic Powder

Diopside  has  been  successfully  prepared  by  a  modified  sol-gel method.Optimization  in calcination temperature and mechanical ball milling  resulted  in  a  pure  and  nano-sized  powder  which characterized by means of scanning electron microscopy (SEM), X- ray diffraction (XRD), transmission electron microscopy (TEM) and fourier  transform  infrared  Spectroscopy  (FT–IR). We  hypo...

full text

Preparation and characterization of ionic liquid functionalized SBA-15 and its application in the synthesis of 2,3-dihydroquinazolinones

N-Methyl-Nʹ-propyltrimethoxysillylimidazolium chloride was prepared as ionic liquid (IL) containing silylating agent and then used for modification of the internal surface of SBA-15 to gain a heterogeneous ionic liquid catalyst. Subsequently, the obtained SBA-IL was characterized using various techniques, including SEM and TEM images, FT-IR, X-ray diffraction, TGA/DTA and BET ...

full text

My Resources

Save resource for easier access later

Save to my library Already added to my library

{@ msg_add @}


Journal title

volume 53  issue 2

pages  169- 176

publication date 2019-12-01

By following a journal you will be notified via email when a new issue of this journal is published.

Hosted on Doprax cloud platform doprax.com

copyright © 2015-2023