Fe3O4@nano-dextrin/Ti(IV) as a bio-based magnetic nano-catalyst for facile synthesis of 2,3-dihydroquinazolin-4(1H)-ones
Authors
Abstract:
A bio-based magnetic nano-catalyst (Fe3O4@nano-dextrin/Ti(IV)) was synthesized via the preparation of Fe3O4@nano-dextrinas magnetic support and then its treatment with titanium tetrachloride (TiCl4). The properties of this catalyst were characterized by different kinds of techniques such as FT-IR, FESEM, TEM, ICP, XRF, VSM and TGA. As a first report, the catalytic activity of Fe3O4@nano-dextrin/Ti(IV) was investigated in the synthesisof 2,3-dihydroquinazolin-4(1H)-ones via condensation between 2-aminobenzamide and aldehyde under mild conditions. Good efficiency, a high percentage of product yields, simplicity of operation and easy recovery and reuse of catalyst are some benefits of this protocol.
similar resources
nano-rods zno as an efficient catalyst for the synthesis of chromene phosphonates, direct amidation and formylation of amines
چکیده ندارد.
Sulfuric Acid Functionalized Magnetic Nanocatalyst for One-pot Green Synthesis of 2,3-Dihydroquinazolin-4 (1H) -ones
Sulfuric acid functionalized magnetic nanocatalyst (SAMNC) has been prepared as an efficientacidic and applied in the one-pot preparation of 2,3-dihydroquinazolin-4 (1H) -one derivatives.This catalyst has been characterized by FT-IR, SEM, and VSM. According to the obtainedresults, including time, yield and recyclability, SAMNC could be considered as an efficient catalystfor organic transformati...
full textsynthesis of amido alkylnaphthols using nano-magnetic particles and surfactants
we used dbsa and nano-magnetic for the synthesis of amido alkylnaphtols.
15 صفحه اولSnCl4/nano-sawdust as an Efficient Bio-based Catalyst for the Synthesis of 2-Substituted Benzothiazoles and Benzimidazoles
SnCl4/nano-sawdust was prepared as a carbohydrate-based catalyst containing of tin bearing cellulose units. The catalyst was characterized by X-ray diffraction (XRD), fourier transform infrared spectroscopy (FT-IR), field emission scanning electron microscopy (FESEM) and energy dispersive X-ray spectroscopy (EDS). The catalyst was applied successfully as a readily available, inexpensive, biodeg...
full textEfficient synthesis of 2,3-dihydroquinazolin-4(1H)-ones using nano-sized protonated ZSM–5 as a biodegradable and reusable solid acid catalyst
Nano-sized protonated ZSM–5 ( H-ZSM-5nanozeolite) was successfully synthesized by the hydrothermal method using the bagasse ash (BGA) as a new silica source. Cultivated BGA in the south of the Caspian Sea (Mazandaran province, Iran) was used for extracting silica powder. H-ZSM-5 was characterized by Fourier transform infrared (FT-IR), X-ray diffraction (XRD), scanning electronic microscopy (SEM...
full textEfficient synthesis of 2,3-dihydroquinazolin-4(1H)-ones using nano-sized protonated ZSM–5 as a biodegradable and reusable solid acid catalyst
Nano-sized protonated ZSM–5 ( H-ZSM-5nanozeolite) was successfully synthesized by the hydrothermal method using the bagasse ash (BGA) as a new silica source. Cultivated BGA in the south of the Caspian Sea (Mazandaran province, Iran) was used for extracting silica powder. H-ZSM-5 was characterized by Fourier transform infrared (FT-IR), X-ray diffraction (XRD), scanning electronic microscopy (SEM...
full textMy Resources
Journal title
volume 10 issue 3
pages 219- 226
publication date 2020-09-01
By following a journal you will be notified via email when a new issue of this journal is published.
Hosted on Doprax cloud platform doprax.com
copyright © 2015-2023