DBU As A Novel and Highly Efficient Catalyst for The Synthesis of 3,5-Disubstituted-2,6-dicyanoanilines Under Conventional and Microwave Conditions

Authors

  • Aman D. Acharya Department of Physics, Lovely Professional University, Phagwara, Punjab, 144411, INDIA
  • Balwant S. Keshwal School of Studies in Chemistry, Vikram University, Ujjain, Madhya Pradesh, 456010, INDIA
  • Deepika Rajguru School of Studies in Chemistry, Vikram University, Ujjain, Madhya Pradesh, 456010, INDIA
Abstract:

3,5-disubstituted-2,6-dicyanoaniline derivatives have been synthesized via the reaction of aryl methylene- and 1-arylethylidenemalonodinitriles using 1,8-diazabicyclo[5.4.0] undec-7-ene (DBU) as a  novel and highly efficient catalyst under conventional as well as microwave conditions. Use of non-hazardous, inexpensive and readily available base catalyst, convenient procedure, short reaction time and improved product yields are some added advantages of the present protocol.

Upgrade to premium to download articles

Sign up to access the full text

Already have an account?login

similar resources

dbu as a novel and highly efficient catalyst for the synthesis of 3,5-disubstituted-2,6-dicyanoanilines under conventional and microwave conditions

3,5-disubstituted-2,6-dicyanoaniline derivatives have been synthesized via the reaction of aryl methylene- and 1-arylethylidenemalonodinitriles using 1,8-diazabicyclo[5.4.0] undec-7-ene (dbu) as a  novel and highly efficient catalyst under conventional as well as microwave conditions. use of non-hazardous, inexpensive and readily available base catalyst, convenient procedure, short reaction tim...

full text

Magnetic Fe3O4 nanoparticles as a highly efficient catalyst for the synthesis of imidazoles under ultrasound irradiation

To be fairly general and catalyst is easily separated by magnetic devices and can be reused without any apparent loss of activity for the reaction. Fe3O4 nanoparticles were prepared by chemical coprecipitation method and was found to be a mild and effective catalyst for the efficient, one-pot, three-component synthesis of 2,4,5-trisubstituted imidazoles at room temperature under ultrasound irra...

full text

Magnetic Fe3O4 nanoparticles as a highly efficient catalyst for the synthesis of imidazoles under ultrasound irradiation

To be fairly general and catalyst is easily separated by magnetic devices and can be reused without any apparent loss of activity for the reaction. Fe3O4 nanoparticles were prepared by chemical coprecipitation method and was found to be a mild and effective catalyst for the efficient, one-pot, three-component synthesis of 2,4,5-trisubstituted imidazoles at room temperature under ultrasound irra...

full text

Melamine trisulfonic acid as a highly efficient catalyst for the synthesis of polyhydroquinolines under solvent-free conditions

A highly efficient, simple and clean solvent-free protocol for the synthesis of polyhydroquinolines is described. The one-pot multi-component condensation reaction between arylaldehydes, dimedone (5,5-dimethylcyclohexane-1,3-dione), β-ketoesters and ammonium acetate in the presence of catalytic amount of (2.5 mol%) melamine trisulfonic acid (MTSA) as a recyclable, green and attractive sulfonic ...

full text

Snail shell as a natural and highly efficient catalyst for the synthesis of imidazole derivatives

A convenient, simple and green process for the synthesis of 2,4,5-triaryl-1H-imidazole and 1,2,4,5-tetraaryl-1H-imidazole derivatives using snail shell, which is abundant in Morocco, as a catalyst in ethanol at 40 °C has been developed. Additionally, short reaction times, excellent yields, simple procedure and relative non-toxicity of the catalyst are other noteworthy advantages and make this m...

full text

My Resources

Save resource for easier access later

Save to my library Already added to my library

{@ msg_add @}


Journal title

volume 35  issue 1

pages  37- 42

publication date 2016-02-01

By following a journal you will be notified via email when a new issue of this journal is published.

Hosted on Doprax cloud platform doprax.com

copyright © 2015-2023