Stir Bar Sorptive Extraction (SBSE) applied to Environmental Aqueous Samples
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منابع مشابه
Analyze Pesticides in Water with Stir Bar Sorptive Extraction and Thermal Separation
Multiple pesticides in water samples were successfully analyzed using an Agilent 5975T LTM GC/MSD equipped with an Agilent J&W DB-5ms Ultra Inert low thermal mass column module, with stir bar sorptive extraction and an Agilent Thermal Separation Probe for sample preparation. The method was simple, rapid, effective, and showed good linearity (R2 >0.9914) and high sensitivity for most of the targ...
متن کاملStir bar sorptive extraction coupled to liquid chromatography-tandem mass spectrometry for the determination of pesticides in water samples: method validation and measurement uncertainty.
Stir bar sorptive extraction followed by liquid desorption and high performance liquid chromatography with tandem mass spectrometry (SBSE-LD-LC-MSMS) has been developed for the determination of 15 pesticides or selected metabolites from different families (herbicides, insecticides, fungicides) in surface water samples. The optimization of parameters that could influence SBSE-LD efficiency was c...
متن کاملA Novel Extraction Procedure for Stir Bar Sorptive Extraction (SBSE): Sequential SBSE for Uniform Enrichment of Organic Pollutants in Water Samples
A novel stir bar sorptive extraction (SBSE) procedure termed sequential SBSE was developed. Compared to conventional SBSE, sequential SBSE provides more uniform enrichment over the entire polarity/volatility range for organic pollutants at ultra-trace levels in water. Sequential SBSE consists of a SBSE performed sequentially on a 5-mL sample fi rst without modifi er using one stir bar, then on ...
متن کاملMulti-Residue Method for the Determination of Five Groups of Pesticides in Non-Fatty Food Samples by Dual Stir Bar Sorptive Extraction (Dual SBSE) and Thermal Desorption GC-MS
A multi-residue method for determination of fi ve groups of 85 pesticides organochlorine, carbamate, organophosphorous, pyrethroid and others in non-fatty food, e.g. vegetables, fruits and green tea is described. The method is based on stir bar sorptive extraction (SBSE) coupled to thermal desorption (TD) and retention time locked (RTL) GC-MS
متن کاملDetermination of Carvedilol Enantiomers in Pharmaceutical Dosages by SBSE-HPLC Based on Diastereomer Formation.
A sensitive, selective and simple method for the simultaneous determination of carvedilol enantiomers in aqueous solution has been developed using stir bar sorptive extraction (SBSE) followed by high-performance liquid chromatography (HPLC) with ultraviolet (UV) detection. This method is based on the reaction of carvedilol enantiomers with (-)-menthyl chloroformate (MCF) after extraction by the...
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